HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenol → 2-(3-chlorophenoxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Reactant | o-Fluorobenzaldehyde | HCID 67970 | — |
| Product | 2-(3-chlorophenoxy)benzaldehyde | HCID 2763428 | 69% |
Reaction Steps
Preparation analogous to Example 12 a) from 2-fluoro-benzaldehyde and 3-chlorophenol. Yield: 69%; yellow oil after bulb tube distillation (150°-180° C., 0.001 torr); 1H-NMR (CDCl3, 200 MHz): 6.92-7.38 (m, 6H); 7.55 (m, 1H); 7.95 (m, 1H), 10.48 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780500 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-163dd8b9b5414889af427d843945f54e |
| Source note | uspto-grants-1998_07 |