HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 18663595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 18663587 | HCID 18663587 | — |
| Product | HCID 18663595 | HCID 18663595 | 45% |
Reaction Steps
Preparation analogous to Example 2 from 10-bromomethyl-7-chloro-dibenz[b,f]oxepine and pyrrolidine. Yield: 45%; melting point: >225° C. decomposition. 1H-NMR (CD3OD, 200 MHz): 1.95-2.20 (m, 4H); 3.25 (m 2H); 3.55 (m, 2H); 4.52 (s, 2H); 7.20-7.45 (m, 7H); 7.60 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780501 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-bca733989ed94f0eb45e13efecffee74 |
| Source note | uspto-grants-1998_07 |