HCID 67572480, compound → HCID 67642996, compound

Participants

Reaction Steps

To a solution of the product from Step F (163 mg, 0.262 mmol) in 3 mL of methanol and 3 mL of EtOAc was added at room temperature 10% palladium on carbon (10 mg). A balloon of hydrogen gas was introduced to the solution via syringe needle, and the reaction was stirred for ca. 20 minutes. The solution was filtered through celite to remove the catalyst, then concentrated in vacuo. The resulting product was purified by silica gel chromatography (4% MeOH/CH2Cl2 with 1% NH4OH) to provide the titled compound (63 mg).

Provenance & Evidence