HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Aspartic Acid → HCID 12991453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Aspartic Acid | HCID 5960 | — |
| Reactant | HCID 12991452 | HCID 12991452 | — |
| Reactant | HCID 86630130 | HCID 86630130 | — |
| Product | HCID 12991453 | HCID 12991453 | — |
Reaction Steps
As a specific example of the HOBT/TBTU Method, when the general procedure is followed, 10 g (24.5 mmole) of BOC-N(Et)Gly-(L)-Asp(OBzl)-OH is used, then 9.3 g of BOC-N(Et)Gly-(L)-Asp(OBzl)-(L)-Cha-NH2 is prepared (96.1 A % pure, 1.77 A % diastereomer at Asp), a 67.7% theoretical yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780590 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-31c2db723c784c12bc03416086711af7 |
| Source note | uspto-grants-1998_07 |