N-(2-Hydroxyethyl)aniline → HCID 86585179, compound

Participants

Reaction Conditions

Reaction Steps

##STR39## 0.283 g of 3-(2-phenyl-2-chloro acetyl) N-methylindole (1 mmole) (H. Nakamura and T. Goto, Heterocyles, 10, 167-170 (1978). and 0.274 g of 2-anilino ethanol (2.0 mmole) were dissolved in 3 ml of dry ethanol and heated in a sealed tube at 80° C. for 8 hours. On cooling the product crystallized out as pale yellow needles which was filtered and dried to yield 0.21 g of N-phenyl indole oxazine Compound 17.

Provenance & Evidence