HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 67675744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl tryptophanate hydrochloride | HCID 2734891 | — |
| Reactant | HCID 67674831 | HCID 67674831 | — |
| Reactant | HCID 67676287 | HCID 67676287 | — |
| Product | HCID 67675744 | HCID 67675744 | — |
Reaction Steps
Following the procedure described in example 12 and starting from N-(3,5-dimethylbenzoyl)-N-ethyl-(D)-phenylalanine (prepared by alkylation of N-(3,5-dimethylbenzoyl)-(D)-phenylalanine methyl ester with ethyl iodide in the presence of sodium hydride followed by hydrolysis of the methyl ester moiety according to example 1 and (L)-tryptophan methyl ester hydrochloride gives N-(3,5-dimethylbenzoyl)-N-ethyl-(D)-phenylalanyl-(L)-tryptophan; FAB-MS m/e 510 (M-H)-.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780498 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-d150c6e1291f4268a2ab292cc9ef9ff3 |
| Source note | uspto-grants-1998_07 |