HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1H-Indole, 2,3-dihydro-3,3-dimethyl-2-methylene-1-octadecyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2,3,3-TRIMETHYLINDOLINE | HCID 10942760 | — |
| Reactant | HCID 21932949 | HCID 21932949 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1H-Indole, 2,3-dihydro-3,3-dimethyl-2-methylene-1-octadecyl- | HCID 11080123 | 84.1% |
Reaction Steps
A mixture of 5.2 g (32 mmol) of 2,3,3-trimethylindoline and 15.8 g (48 mmol) of octadecylammonium bromide was heated with stirring followed by treating with a solution of 8 g of sodium hydroxide in 50 ml of water. After usual working-up, there were obtained 4.2 g of the title compound in a 84.1% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05782969 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-cfd9262709cd4727a6d4a6aa9eb72577 |
| Source note | uspto-grants-1998_07 |