HCID 136351314, compound → HCID 135848335, compound
Reaction equation
ClC1C=C([N+]([O-])=O)C=CC=1N=NC1C=C(C)C(N=NC2C3C(=CC=CC=3)C=C(NC3C=CC=CC3=C=O)C=2O)=CC=1[S:42]([F:45])(=[O:44])=[O:43].C[C:47]1[CH:52]=[CH:51][C:50](S(F)(=O)=O)=[CH:49][C:48]=1[N:57]=[N:58][C:59]1[CH:64]=[CH:63][C:62]([N:65]=[N:66][C:67]2[C:76]3[C:71](=CC=CC=3)[CH:70]=[C:69](NC3C=CC=CC3=C=O)[C:68]=2O)=[C:61]([O:87][CH2:88]C)[CH:60]=1.FS(C1C=C(N=NC2C=C(OC)C(N=NC3C4C(=CC=CC=4)C=C(NC4C5C(=CC=CC=5)C=CC4=C=O)C=3O)=CC=2OC)C=CC=1)(=O)=[O:92].CC1C=CC(S(F)(=O)=O)=CC=1N=NC1C2C(=CC=CC=2)C(N=NC2C3C(=CC=CC=3)C=C(NC3C=CC=CC3=C=O)C=2O)=CC=1>>[OH:92][C:70]1[CH:69]=[CH:68][C:67]([N:66]=[N:65][C:62]2[CH:63]=[CH:64][C:59]([N:58]=[N:57][C:48]3[CH:49]=[CH:50][C:51]([S:42]([F:45])(=[O:44])=[O:43])=[CH:52][CH:47]=3)=[CH:60][C:61]=2[O:87][CH3:88])=[CH:76][CH:71]=1Participants
5
Procedure
1-(2-chloro-4-nitrophenylazo)-5-methyl-2-fluorosulphonyl-4-(2-hydroxy-3-(carbonyl (N-phenyl) amino) naphth-1-ylazo) benzene; 1-(2-methyl-5-fluorosulphonylphenylazo)-3-ethoxy-4-(2-hydroxy-3-(carbonyl (N-phenyl) amino) naphth-1-ylazo) benzene; 1-(3-fluorosulphonylphenylazo)-2,5-dimethoxy-4-(2-hydroxy-3-(carbonyl(N-naphth-1-yl)amino)naphth-1-ylazo)benzene; and 1-(2-methyl-5-fluorosulphonylphenylazo)-4-(2-hydroxy-3-(carbonyl(N-phenyl)amino)naphth-1-ylazo)naphthalene and these form a further feature of the present invention.
Sources & evidence
- ORD record
- ord-26170b7564f84bfbb84ca7b490d3912b
- Source dataset
- uspto-grants-1998_07
- Patent number
- US05782934
Reaction notes
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