HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19068921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 19068922 | HCID 19068922 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19068921 | HCID 19068921 | — |
Reaction Steps
To a solution of 2,3,3a,4-tetrahydro-2-(5-methyl-1H-imidazol-4-yl)methyl-1H-imidazo[5, 1-c] [1,4]benzoxazin-1-one (0.5 g; 0.00176 moles) in absolute ethanol (10 ml), an excess of a solution of hydrochloric acid is added. Diethyl ether is added, the precipitate is filtered to give 0.52 g of the title product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05783574 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-da0e93a00b3e4dc796aa11535fff3cc3 |
| Source note | uspto-grants-1998_07 |