Aluminum(III) Chloride → HCID 19068990, compound

HRID 1957197Notes

Reaction equation

HRID 1957197 reaction equation
C([N:8]1[C:16]2[C:11](=[CH:12][C:13]([Br:17])=[CH:14][CH:15]=2)[C:10]2[CH:18]=[C:19]([C:21]([O:23][CH3:24])=[O:22])[S:20][C:9]1=2)C1C=CC=CC=1.[Al+3].[Cl-].[Cl-].[Cl-].S1C2NC3C(C=2C=C1C(OC)=O)=CC=CC=3>>[Br:17][C:13]1[CH:12]=[C:11]2[C:16](=[CH:15][CH:14]=1)[NH:8][C:9]1[S:20][C:19]([C:21]([O:23][CH3:24])=[O:22])=[CH:18][C:10]2=1

Participants

4

Reactant 3

HCID 6451240Aluminum(III) ChlorideHCID 10681031HCID 10681031, compoundHCID 19068970HCID 19068970, compound

Product 1

HCID 19068990HCID 19068990, compoundYield 19.4%

Procedure

Prepared from (39) (1 g) by means of AlCl3 (2 g) as described for (19) gave 0.15 g of (41), m.p. 216°-218° C.

Sources & evidence

ORD record
ord-84123523b27d4e07b4f31a6e8fbd2f02
Source dataset
uspto-grants-1998_07
Patent number
US05783575

Reaction notes

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