Potassium Hydroxide → HCID 19068949, compound

HRID 1957210Notes

Reaction equation

HRID 1957210 reaction equation
[OH-].[K+].[Cl:3][C:4]1[CH:5]=[CH:6][CH:7]=[C:8]2[C:12]=1[N:11]([CH3:13])[C:10]1[S:14][C:15]([C:17]([O:19]C)=[O:18])=[CH:16][C:9]2=1>>[Cl:3][C:4]1[CH:5]=[CH:6][CH:7]=[C:8]2[C:12]=1[N:11]([CH3:13])[C:10]1[S:14][C:15]([C:17]([OH:19])=[O:18])=[CH:16][C:9]2=1

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 19068977HCID 19068977, compound

Product 1

HCID 19068949HCID 19068949, compoundYield 99.3%

Procedure

Prepared from KOH (4.73 g), (50) (5.9 g) after reflux overnight yielding (57) 5.54 g (99.3%). M.p. 233°-234° C.

Workup

  1. temperatureafter reflux overnight

Sources & evidence

ORD record
ord-62efc9141a834b02b38867c315fa04fb
Source dataset
uspto-grants-1998_07
Patent number
US05783575

Reaction notes

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