Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | HCID 18704208 | HCID 18704208 | — |
| Reactant | HCID 19598386 | HCID 19598386 | — |
| Product | HCID 19598372 | HCID 19598372 | — |
Reaction Steps
2.1 ml (15 mmol) of triethylamine in 10 ml of tetrahydrofuran are added dropwise at 25° C. to a solution of 1.5 g (4 mmol) of N-(4-benzyloxycarbonylphenyl)-4-toluenesulfonamide, 1.23 g (4.4 mmol) of acridinecarbonyl chloride hydrochloride and 0.02 g of dimethylaminopyridine in 20 ml of anhydrous tetrahydrofuran. The temperature is raised to 600° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05783696 |
|---|
| Source dataset | uspto-grants-1998_07 |
|---|
| ORD ID | ord-7f9d6b98b44147b0ae593d7420a551e8 |
|---|
| Source note | uspto-grants-1998_07 |
|---|
