HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 2-amino-6-chlorobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Amino-6-chlorobenzoic acid | HCID 75071 | — |
| Product | Methyl 2-amino-6-chlorobenzoate | HCID 592849 | 78.4% |
Reaction Steps
Using the procedure described above in Preparation 1, 5.0 g (0.029 mol) of 6-chloroanthranilic acid and 2.75 ml (0.044 mol) of iodomethane were reacted in the presence of 4.08 g (0.073 mol) of powdered potassium hydroxide to give 4.22 g (78%) of methyl 6-chloroanthranilate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05783589 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-5b67cfff2a9f419b85caca3633b223c8 |
| Source note | uspto-grants-1998_07 |