HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1957460Generated: November 1, 2026
Azobisisobutyronitrile → HCID 86752933, compound
https://huagongshe.com/reaction/1957460
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Methylhydroquinone | HCID 7253 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Solvent | Hexane | HCID 8058 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86752933 | HCID 86752933 | — |
Reaction Steps
2-isopropenyl AQ (0.3 g), 0.5 g acrylic acid and 0.7 g methyl acrylate (Aldrich) containing inhibitor (200 ppm methyl hydroquinone, MeHQ) and 40 mg 2,2'-azobis-isobutyronitrile (AIBN) were placed in a heavy-walled glass tube. Oxygen was removed by three freeze/thaw cycles. The tube was sealed and heated to 80° C. for 1 h. The polymer thus obtained was dissolved in dioxane. TLC (20% AcOEt in hexane) shows disappearance of free isopropenyl AQ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05785943 |
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| Source dataset | uspto-grants-1998_07 |
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| ORD ID | ord-026a17011926448b924123aec94375dd |
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| Source note | uspto-grants-1998_07 |
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