HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 19067674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,5-Difluoro-4-nitrophenol | HCID 2782490 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19067674 | HCID 19067674 | 44.2% |
Reaction Steps
The product of step (a) (3.4 g, 20 mmol), 50 ml acetonitrile, 3.3 g potassium carbonate and 3 g allyl bromide were combined, heated to reflux for one hour and stripped. The mixture was extracted with dichloromethane, treated with water and separated. The organics were dried over magnesium sulfate and stripped to yield 1.9 g of 4-allyloxy-2,5 difluoro nitrobenzene product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05786301 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-5a6188f88c15440e8b2e78913674161a |
| Source note | uspto-grants-1998_07 |