Trifluoroacetic acid → HCID 86752941, compound

Participants

Reaction Steps

A 3 g of this di-t-butyl dioleylmalonate was dissolved in a solution comprising 20 ml of anisole, 20 ml of dichloromethane and 10 ml of trifluoroacetic acid, followed by stirring at room temperature overnight. After reaction, volatile components were distilled off. The residue was then heated at 150° C. for 4 hours to remove carbonic acid, thereby obtaining 2.32 g of α,α-dioleylacetic acid [RF =0.12 (chloroform:methanol=10:1)].

Provenance & Evidence