beta-Cyclocitral → HCID 60135426, compound

HRID 1957885Notes

Reaction equation

HRID 1957885 reaction equation
[CH3:1][C:2]1[CH2:7][CH2:6][CH2:5][C:4]([CH3:9])([CH3:8])[C:3]=1[CH:10]=O.CC1(C)CCCC(C)C1CC[CH2:22][C:23]([OH:25])=[O:24].CC1(C)C(C)CCC1CCCC(O)=O>>[CH3:9][C:4]1([CH3:8])[CH2:5][CH2:6][CH2:7][CH:2]([CH3:1])[CH:3]1[CH2:10][CH2:22][C:23]([OH:25])=[O:24]

Participants

4

Reactant 3

HCID 9895beta-CyclocitralHCID 250998174-(2,2,3-Trimethylcyclopentyl)butanoic acidHCID 25221164HCID 25221164, compound

Product 1

HCID 60135426HCID 60135426, compound

Procedure

3-(2,2,6-trimethylcyclohexyl)propanoic acid was synthesized in three steps starting from 2,6,6-trimethylcyclohex-1-enecarbaldehyde, analogous to the 3-step procedure described for 4-(2,2,6-trimethylcyclohexyl)butanoic acid and 4-(2,2,3-trimethylcyclopentyl)butanoic acid herein-above, as indicated below.

Sources & evidence

ORD record
ord-fe0bcc1ac6b841a6b775509ee43b888b
Source dataset
uspto-grants-2013_04
Patent number
US08409649B2

Reaction notes

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