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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1957919Generated: November 2, 2026

HCID 13634747, compound → 1-Butanol, 2-[(4-methylphenyl)methylene]-, (2E)-

https://huagongshe.com/reaction/1957919

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13634747HCID 13634747—
ReactantAluminium lithium hydrideHCID 21226445—
SolventDiethyl EtherHCID 3283—
Product1-Butanol, 2-[(4-methylphenyl)methylene]-, (2E)-HCID 67151062—

Reaction Conditions

Temperature-78 °C

Reaction Steps

LiAlH4 (1.15 g, 30 mmol) was added to a diethyl ether (100 ml) solution of (E)-2-ethyl-3-(4-methylphenyl)-2-propenal (5.0 g, 28.7 mmol) cooled in a −78° C. cold bath.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08410042B2
Source datasetuspto-grants-2013_04
ORD IDord-705704abc66a42a6a4f444551d081ebe
Source noteuspto-grants-2013_04