反应详情

1-methanesulfonyl-3-nitro-5-trifluoromethylbenzene (500 mg; 1.9 mmol) was dissolved in 100 mL methanol, 70 mg of Pd/C (10%) was added and the mixture was hydrogenated at 3 bar. The reaction mixture was filtrated and solvent removed under reduced pressure. 250 mg (1.04 mmol; 55% yield) of a colorless solid were obtained.

1. filtrationThe reaction mixture was filtrated
2. customsolvent removed under reduced pressure
3. custom250 mg (1.04 mmol; 55% yield) of a colorless solid were obtained