HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-[(3-nitrophenyl)sulfonyl]- → Ethanol, 2-[(3-aminophenyl)sulfonyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-[(3-nitrophenyl)sulfonyl]- | HCID 170561 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Ethanol, 2-[(3-aminophenyl)sulfonyl]- | HCID 78905 | 100% |
Reaction Steps
2-(3-Nitrophenylsulfonyl)ethanol (10 g; 43 mmol) was dissolved in 200 ml tetrahydrofuran and 200 mL ethanol, 3 g Pd/C (10%) was added and the mixture treated with hydrogen gas. The solvents were removed to obtain 8.8 g (43 mmol, 100% yield) of the desired compound as colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410100B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-a6be3af4b8a14c029b91e3013374c2bb |
| Source note | uspto-grants-2013_04 |