Morpholine → HCID 68425046, compound

HRID 1957979Notes

Reaction equation

HRID 1957979 reaction equation
[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][S:5]([C:8]1[CH:9]=[C:10]([CH:12]=[CH:13][CH:14]=1)[NH2:11])(=[O:7])=[O:6].N1C[CH2:20][O:19][CH2:18]C1>>[N:2]1([CH2:3][CH2:4][S:5]([C:8]2[CH:9]=[C:10]([NH:11][C:8]3[CH:9]=[CH:10][CH:12]=[CH:13][CH:14]=3)[CH:12]=[CH:13][CH:14]=2)(=[O:7])=[O:6])[CH2:15][CH2:18][O:19][CH2:20][CH2:1]1

Participants

3

Reactant 2

HCID 8083MorpholineHCID 21424576HCID 21424576, compound

Product 1

HCID 68425046HCID 68425046, compoundYield 98.7%

Procedure

This aniline was prepared with the same procedure described for the preparation of 3-(2-Dimethylaminoethylsulfonyl)-aniline, using morpholine instead of dimethylamine. 770 mg (2.137 mmol; 98.7% yield) were obtained.

Workup

  1. custom770 mg (2.137 mmol; 98.7% yield) were obtained

Sources & evidence

ORD record
ord-c7c2a5fa2814484e87d70c45ba27b007
Source dataset
uspto-grants-2013_04
Patent number
US08410100B2

Reaction notes

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