HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-1H-pyrazole-4-carboxylic acid → N-(2-Fluoroethyl)-N,1-dimethyl-1H-pyrazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-1H-pyrazole-4-carboxylic acid | HCID 643160 | — |
| Reactant | (2-Fluoro-ethyl)-methyl-amine hydrochloride | HCID 85799809 | — |
| Product | N-(2-Fluoroethyl)-N,1-dimethyl-1H-pyrazole-4-carboxamide | HCID 58446960 | — |
Reaction Steps
From 1-methyl-1H-pyrazole-4-carboxylic acid (1.0 g, 7.93 mmol) and 2-fluoro-N-methylethanamine hydrochloride (991 mg, 8.72 mmol). Yellow oil (1.41 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410117B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-f947428ab4d64aeeb7ce22a81e8ad4f3 |
| Source note | uspto-grants-2013_04 |