Potassium Carbonate → HCID 44626131, compound

Participants

Reaction Conditions

Reaction Steps

1.65 g of the compound obtained in stage 1G), 0.57 g of K2CO3 and 0.83 g of 3-chloropropan-1-ol are added to 10 ml of DMF. The reaction medium is heated at 90° C. for 3 hours. The reaction medium is then poured onto distilled water and the expected compound is extracted with ethyl acetate. The organic phase is dried and evaporated. After crystallizing in ethyl acetate, 1.2 g of the expected compound are obtained.

Provenance & Evidence