HRID1958732
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of (R)-benzyl 4-(dimethylamino)-3-(5-(1-methyl-3-(trifluoromethyl)-1H-pyrazol-5-yl)thiophene-2-sulfonamido)butanoate in CH2Cl2 (2 mL) was added methyl iodide (100 μL). The reaction was stirred overnight and concentrated to dryness to give the title compound in quantitative yield.
WORKUP
后处理
- concentrationconcentrated to dryness