HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Decylbenzene-1-sulfonyl chloride → (R)-benzyl 3-(4-decylphenylsulfonamido)-4-(dimethylamino)butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Decylbenzene-1-sulfonyl chloride | HCID 12582787 | — |
| Reactant | (R)-benzyl 3-amino-4-(dimethylamino)butanoate | HCID 46223508 | — |
| Product | (R)-benzyl 3-(4-decylphenylsulfonamido)-4-(dimethylamino)butanoate | HCID 86641229 | 94% |
Reaction Steps
According to the method described in example S72a, (R)-benzyl 3-amino-4-(dimethylamino)butanoate (27 mg, 0.086 mmol) was reacted with 4-decylbenzene-1-sulfonyl chloride to yield the title compound as a white solid (50 mg, 94%). MS ESI 517.4 [M+H]+, calcd for [C29H44N2O4S+H]+ 517.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410150B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-43de5c4380374e30ae9c9f813e6379c3 |
| Source note | uspto-grants-2013_04 |