HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → HCID 86641231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | HCID 59294388 | HCID 59294388 | — |
| Product | HCID 86641231 | HCID 86641231 | 87% |
Reaction Steps
According to the method described in example S76a, (R)-benzyl 3-(5-bromothiophene-2-sulfonamido)-4-(dimethylamino)butanoate was reacted with ethynylbenzene to give the title compound as a brown oil (55 mg, 87%). MS ESI 483.3 [M+H]+, calcd for [C25H26N2O4S2+H]+ 483.13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410150B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-c5d201e897e04e5dab17a1d55e400fd4 |
| Source note | uspto-grants-2013_04 |