HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Ethynyltoluene → HCID 86641232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Ethynyltoluene | HCID 13018 | — |
| Reactant | HCID 59294388 | HCID 59294388 | — |
| Product | HCID 86641232 | HCID 86641232 | 89% |
Reaction Steps
According to the method described in example S76a, (R)-benzyl 3-(5-bromothiophene-2-sulfonamido)-4-(dimethylamino)butanoate was reacted with p-ethynyltoluene to give the title compound as a black oil (55 mg, 89%). MS ESI 497.3 [M+H]+, calcd for [C26H28N2O4S2+H]+ 497.15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410150B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1a37f9665bd345b48a414ff3a0a78f09 |
| Source note | uspto-grants-2013_04 |