HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Formyl-4-methylbenzoic acid → HCID 86650509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Formyl-4-methylbenzoic acid | HCID 19019191 | — |
| Reactant | HCID 178418750 | HCID 178418750 | — |
| Product | HCID 86650509 | HCID 86650509 | — |
Reaction Steps
The title compound is prepared in analogy to 3-formyl-4-methyl-benzoic acid using diethyl zinc in step b). LC-MS*: tR=0.45 min, [M−H]−=177.30; 1H NMR (D6-DMSO): δ 1.21 (t, J=7.5 Hz, 3H), 3.10 (q, J=7.5 Hz, 2H), 7.53 (d, J=8.0 Hz, 1H), 8.11 (dd, J=7.8, 1.5 Hz, 1H), 8.39 (d, J=1.3 Hz, 1H), 10.30 (s, 1H), 13.10 (br s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410151B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-9c09280a4b994daba69e92c8d92dbf8a |
| Source note | uspto-grants-2013_04 |