2,4-Difluorophenylboronic acid → HCID 59443034, compound

HRID 1959153Notes

Reaction equation

HRID 1959153 reaction equation
Cl[C:2]1[C:7]2[CH:8]=[CH:9][C:10]([N+:12]([O-:14])=[O:13])=[CH:11][C:6]=2[O:5][C:4]([CH2:17][CH3:18])([CH2:15][CH3:16])[N:3]=1.[F:19][C:20]1[CH:25]=[C:24]([F:26])[CH:23]=[CH:22][C:21]=1B(O)O>>[CH2:15]([C:4]1([CH2:17][CH3:18])[N:3]=[C:2]([C:23]2[CH:22]=[CH:21][C:20]([F:19])=[CH:25][C:24]=2[F:26])[C:7]2[CH:8]=[CH:9][C:10]([N+:12]([O-:14])=[O:13])=[CH:11][C:6]=2[O:5]1)[CH3:16]

Participants

3

Reactant 2

HCID 27343342,4-Difluorophenylboronic acidHCID 68483656HCID 68483656, compound

Product 1

HCID 59443034HCID 59443034, compound

Procedure

The compound obtained in (3) described above (1.0 g) and 2,4-difluorophenylboronic acid (1.2 g) were treated in the same manner as Reference Example 39(2) to give the titled compound (0.6 g) as a yellow oil.

Sources & evidence

ORD record
ord-c4cd6fcce1004eebae297e1a248d07fd
Source dataset
uspto-grants-2013_04
Patent number
US08410166B2

Reaction notes

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