HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydro-4H-pyran-4-ol → HCID 66730495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydro-4H-pyran-4-ol | HCID 74956 | — |
| Reactant | 2-[4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]ethyl benzenesulfonate | HCID 86661967 | — |
| Product | HCID 66730495 | HCID 66730495 | 68.3% |
Reaction Steps
Using tetrahydropyran-4-ol (3.7 g, 36.2 mmol) and 2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]ethyl benzenesulfonate (6 g, 14.3 mmol) synthesized in Reference Example 2 (2c), the desired title compound (3.4 g, yield 68%) was obtained by the same method as in Reference Example 2 (2a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410273B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-2222230fa55247eb89b67f1dcf2c4251 |
| Source note | uspto-grants-2013_04 |