HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 57861230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 57861231 | HCID 57861231 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 57861230 | HCID 57861230 | — |
Reaction Steps
A mixture of N-(3-methylquinoxalin-2-yl)-N-(cyclopentylmethyl)ethylamine (160 mg, 0.59 mmol), N-bromosuccinimide (130 mg, 0.73 mmol), and 2,2′-azobisisobtyronitrile (10 mg) in CCl4 is stirred and refluxed for 1 hour. The reaction mixture is purified by silica gel column chromatography to give N-[3-(bromomethyl)quinoxalin-2-yl]-N-(cyclopentylmethyl)ethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410275B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-90ab4c9cc5d04f838f839a759eba3ed3 |
| Source note | uspto-grants-2013_04 |