HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → 1-Undecanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Undecanoic Acid | HCID 8180 | — |
| Product | 1-Undecanol | HCID 8184 | 22% |
Reaction Steps
In 3 mL of acetic acid was dissolved 375 mg of 1-undecanol to give a solution, and the solution was combined with 150 mg of the catalyst B10 obtained from Example 22 and 32 mg of N-hydroxyphthalimide, followed by stirring at 100° C. in an oxygen atmosphere at normal atmospheric pressure for 4 hours. The reaction mixture was analyzed through gas chromatography to find that undecanoic acid was produced in a yield of 22% with a conversion from 1-undecanol of 44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410308B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-39b102dd695a4a609d28c2f46874fe36 |
| Source note | uspto-grants-2013_04 |