HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyltin iodide → Tributyltin fluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyltin iodide | HCID 23765 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Product | Tributyltin fluoride | HCID 16120 | — |
Reaction Steps
Bu3SnI will react on the column with KF to give Bu3SnF, which rapidly reacts with the silica. The purified product in ether is recovered and then dried on a vane pump. Bu3SnI+KFaq→Bu3SnF↓+Klaq
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415016B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1a06191fa37f42d6922cccb6a3900418 |
| Source note | uspto-grants-2013_04 |