HRID1961478

反应详情

EQUATION

反应方程式

HRID 1961478 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

6-(Benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide (62.0 mg, 0.14 mmol) was dissolved in MeOH (2 ml). Pd (C) (3.1 mg) was added to the solution. The mixture was hydrogenated at atmospheric pressure for 24 h. Then it was filtered through a pad of celite and concentrated under reduced pressure. The residue was washed with CH2Cl2 yielding 37 mg (76%) of the title compound.

WORKUP

后处理

  1. filtrationThen it was filtered through a pad of celite
  2. concentrationconcentrated under reduced pressure
  3. washThe residue was washed with CH2Cl2 yielding 37 mg (76%) of the title compound