HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyborohydride → HCID 66627995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyborohydride | HCID 2724942 | — |
| Reactant | HCID 15105361 | HCID 15105361 | — |
| Reactant | HCID 178453924 | HCID 178453924 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 66627995 | HCID 66627995 | — |
Reaction Steps
The title compound was prepared from ((4-Fluoro-phenyl)-(4-hydroxy-piperidin-4-yl)-methanone and trans-[4-(2-Oxo-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester according to the procedure described for the synthesis of (4-{2-Trans-[4-(4-Fluoro-benzoyl)-piperidin-1-yl]-ethyl}-cyclohexyl)-carbamic acid tert-butyl ester (intermediate E, example 1) in 1,2 dichloroethane using triacetoxyborohydride. MS (m/e): 451.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415350B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-af688e31b52f4fa69bc1651eccf68ff1 |
| Source note | uspto-grants-2013_04 |