HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Nitrophenyl)propionitrile → 10139-91-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Nitrophenyl)propionitrile | HCID 5051805 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 10139-91-0 | HCID 10419324 | — |
Reaction Steps
3-(4-Nitrophenyl)propionitrile (38) (740 mg, 4.2 mmol) was reduced by using procedure described in Example 5 in methanol (100 mL) with 10% Pd/C as a catalyst to afford 3-(4-aminophenyl)propionitrile (39). 1H NMR (DMSO-d6): δ 6.91-6.88 (d, J=9.0 Hz, 2H), 6.49-6.46 (d, J=9.0 Hz, 2H), 4.92 (s, 2H), and 2.66 (s, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415365B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-30d9e5ded9374cfe8384f3a3b82a305a |
| Source note | uspto-grants-2013_04 |