HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-3-fluoro-2-methylaniline → (5-Bromo-3-fluoro-2-methyl-phenyl)-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-3-fluoro-2-methylaniline | HCID 2737640 | — |
| Reactant | 2-(5-Bromo-4-fluoro-2-methylphenyl)acetic acid | HCID 59614601 | — |
| Product | (5-Bromo-3-fluoro-2-methyl-phenyl)-acetic acid | HCID 58083211 | — |
Reaction Steps
(5-Bromo-3-fluoro-2-methyl-phenyl)-acetic acid was prepared analogously to the synthesis of (5-bromo-4-fluoro-2-methyl-phenyl)-acetic acid (preparation example P5, step P5.3) starting from 5-bromo-3-fluoro-2-methyl-phenylamine (preparation example P7, step P7.1) by making use of the procedures described under step P5.1, step P5.2 and step P5.3. The title acid was obtained as a solid, mp: 147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415369B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-3cf5c538ee0f48f39629e0148c3f5e9f |
| Source note | uspto-grants-2013_04 |