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HRID1962895

反应详情

EQUATION

反应方程式

HRID 1962895 的结构方程式

REACTANTS

反应物

2
结构：FC(F)(F)c1cc(-c2ccc(Cl)s2)nc(Cl)n1
HCID86624627

未命名化合物

结构：Ic1c[nH]cn1
HCID178506559

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)(F)c1cc(-c2ccc(Cl)s2)nc(-n2cnc(I)c2)n1
HCID67393367

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 2-chloro-4-(5-chloro-thiophen-2-yl)-6-trifluoromethyl-pyrimidine (example A.1) (1.2 g, 4.0 mmol) and commercially available 4-iodo-imidazole (0.85 g, 4.4 mmol) according to the general procedure IIa. Obtained as an off-white solid (1.78 g, 97%). MS (ISP) 457.0 [(M+H)+]; mp 251° C.