HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium periodate → HCID 66732469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 66732003 | HCID 66732003 | — |
| Catalyst | Ruthenium trichloride | HCID 61850 | — |
| Product | HCID 66732469 | HCID 66732469 | — |
Reaction Steps
The compound was prepared as described in Reference Compound 4, Step 5 starting from methyl 4-(hydroxymethyl)-2-methylpiperidine-1-carboxylate, sodium periodate (3.53 g, 16.5 mmol) and ruthenium(III) chloride (0.025 g, 0.12 mmol), which resulted in the title compound. MS m/z 200 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415378B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-c0830a7463fa416b8b3ba768e004a639 |
| Source note | uspto-grants-2013_04 |