HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-{4-[4-(methylamino)-3-nitrophenoxy](2-pyridyl)}-2-(4-methylpiperidyl)acetamide → N-{4-[3-amino-4-(methylamino)phenoxy](2-pyridyl)}-2-(4-methylpiperidyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-{4-[4-(methylamino)-3-nitrophenoxy](2-pyridyl)}-2-(4-methylpiperidyl)acetamide | HCID 59790224 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | N-{4-[3-amino-4-(methylamino)phenoxy](2-pyridyl)}-2-(4-methylpiperidyl)acetamide | HCID 59789988 | — |
Reaction Steps
N-{4-[4-(methylamino)-3-nitrophenoxy] (2-pyridyl)}-2-(4-methylpiperidyl)acetamide was hydrogenated in the presence of Pd C for 4 hours. The catalyst was removed via filtration and filtrate was concentrated to give N-{4-[3-amino-4-(methylamino)phenoxy](2-pyridyl)}-2-(4-methylpiperidyl)acetamide. MS: MH+=370.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415382B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-42ace8d8c13b4cc98b0a1e15ce1e5de7 |
| Source note | uspto-grants-2013_04 |