HRID1963746

反应详情

EQUATION

反应方程式

HRID 1963746 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To 3-(2-fluoro-5-nitrophenyl)-tetrahydro-3-methylfuran in methanol was added a catalytic amount of palladium on carbon (10%). The mixture was allowed to stir for 1 h at room temperature under hydrogen atmosphere. Mixture was filtered though celite and concentrated to afford 4-fluoro-3-(tetrahydro-3-methylfuran-3-yl)benzenamine.

WORKUP

后处理

  1. filtrationMixture was filtered though celite and
  2. concentrationconcentrated