HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclododecanamine → 5-Chloro-2-[(([2-(cyclododecylamino)-2-oxoethyl]sulfanyl)acetyl)amino]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclododecanamine | HCID 2897 | — |
| Reactant | [(2-([4-Chloro-2-(methoxycarbonyl)phenyl]amino)-2-oxoethyl)sulfanyl]acetic acid | HCID 51040153 | — |
| Product | 5-Chloro-2-[(([2-(cyclododecylamino)-2-oxoethyl]sulfanyl)acetyl)amino]benzoic acid | HCID 44250627 | — |
Reaction Steps
Using the same method as in Example 1-(ii), cyclododecylamine was reacted with the [(2-([4-chloro-2-(methoxycarbonyl)phenyl]amino)-2-oxoethyl)sulfanyl]acetic acid obtained in Example 12-(i) to give 5-chloro-2-[(([2-(cyclododecylamino)-2-oxoethyl]sulfanyl)acetyl)amino]benzoic acid.methyl ester (yield: 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415479B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-2a81bad3b65142baa17296efccaf7681 |
| Source note | uspto-grants-2013_04 |