2-(Furan-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane → HCID 86653352, compound

HRID 1964053Notes

Reaction equation

HRID 1964053 reaction equation
CC1(C)C(C)(C)OB([C:9]2[CH:13]=[CH:12][O:11][CH:10]=2)O1.Br[C:16]1[CH:17]=[C:18]([CH:24]=[CH:25][CH:26]=1)[CH2:19][NH:20][C:21](=[O:23])[OH:22]>>[O:11]1[CH:12]=[CH:13][C:9]([C:16]2[CH:17]=[C:18]([CH:24]=[CH:25][CH:26]=2)[CH2:19][NH:20][C:21](=[O:22])[OH:23])=[CH:10]1

Participants

3

Reactant 2

HCID 27739962-(Furan-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneHCID 21712818HCID 21712818, compound

Product 1

HCID 86653352HCID 86653352, compound

Procedure

Using the same method as in Example 5-(i), 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)furan was reacted with the (3-bromobenzyl)carbamic acid.tert-butyl to give [3-(furan-3-yl)benzyl]carbamic acid.tert-butyl (yield: 96%).

Sources & evidence

ORD record
ord-ffe67869fbef4506b53da1314a5f046e
Source dataset
uspto-grants-2013_04
Patent number
US08415479B2

Reaction notes

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