Methyldichlorosilane → HCID 75237368, compound

Participants

Reaction Steps

In the same manner as that of Embodiment 1, 80 g (0.50 mol) of vinyltrichlorosilane, 171.4 g (1.49 mol) of methyldichlorosilane, and 14.7 g of tetrabutylphosphonium chloride were put in a 500 ml stainless steel tube and reacted at 180° C. for six hours. The reactant was vacuum-distilled to obtain 61.4 g (yield: 51.2%) of 2,5-bis(methyldichlorosilyl)-1,1,4,4-tetrachloro-1,4-disilacyclohexane. The obtained product was analyzed with 300 MHz 1H magnetic resonance.

Provenance & Evidence