(Boc-aminooxy)acetic acid → HCID 46193807, compound

HRID 1964787Notes

Reaction equation

HRID 1964787 reaction equation
[C:1]([NH:8][O:9][CH2:10][C:11]([OH:13])=[O:12])([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2]>C(OC(=O)C)(=O)C>[C:1]([NH:8][O:9][CH2:10][C:11]([O:13][C:11](=[O:12])[CH2:10][O:9][NH:8][C:1]([O:3][C:4]([CH3:6])([CH3:5])[CH3:7])=[O:2])=[O:12])([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2]

Participants

3

Reactant 1

HCID 2755974(Boc-aminooxy)acetic acid

Product 1

HCID 46193807HCID 46193807, compound

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

A further embodiment of the invention according to the above reaction of obtaining formula (A) is dissolving (Boc-aminoxy)acetic acid, (G), in acetic anhydride and heating the mixture to a temperature in the range of about 40° C. to about 70° C. for about 48 hours to about 72 hours to form (Boc-aminooxy)acetic anhydride, (H).

Workup

  1. customA further embodiment of the invention according to the above reaction
  2. temperatureheating the mixture to a temperature in the range of about 40° C. to about 70° C. for about 48 hours to about 72 hours

Sources & evidence

ORD record
ord-46f875f63ab44e48923b1182ad8ddb90
Source dataset
uspto-grants-2013_04
Patent number
US08415510B2

Reaction notes

Loading…