HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzylamine → HCID 60036794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzylamine | HCID 66648 | — |
| Reactant | (1,1'-Biphenyl)-4-sulphonyl chloride | HCID 74192 | — |
| Reactant | 3-(tert-Butoxycarbonyl)-1,3-thiazolidine-2-carboxylic acid | HCID 4644094 | — |
| Reactant | Benzophenone, 4-nitro-, oxime | HCID 6506582 | — |
| Product | HCID 60036794 | HCID 60036794 | — |
Reaction Steps
Following the general solid phase method as outlined Example 33, starting from 3-(tert-butoxycarbonyl)-1,3-thiazolidine-2-carboxylic acid, Kaiser oxime resin, 1,1′-biphenyl-4-sulfonyl chloride and (2-chlorophenyl)methanamine, the title compound was obtained in 85% purity by HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415480B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-9b7f46b1182041b5ae79664ad140fc5d |
| Source note | uspto-grants-2013_04 |