Hydrochloric Acid → HCID 178524574, compound

Participants

Reaction Steps

Methyl 2-(2-hydroxypyridin-3-yl)-5-nitrobenzoate (Reference Compound No. 1-3-(2), 300 mg, 1.09 mmol) was dissolved in methanol (2 mL), then conc. HCl (5 mL) was added thereto, and then the reaction mixture was refluxed overnight. The solvent was removed under reduced pressure to give the titled reference compound (263 mg) as a yellow solid. (Yield 93%)

Provenance & Evidence