Water → (8-Bromo-2-methylquinolin-4-yl)-(3,4-dichlorobenzyl)-amine

Beteiligte Stoffe

Reaktionsschritte

8-Bromo-4-chloro-2-methylquinoline (4.50 g, 17.5 mmole) and 3,4-dichlorobenzylamine (6.30 g, 35.8 mmole) in dimethylsulfoxide (6 mL) were stirred at 140° C. for 2 h in a microwave oven. Water was added and the mixture was decanted to obtain an oily residue. The residue was washed with ethyl acetate to give a white solid (1.40 g, 20%).

Herkunft & Nachweise