HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2,2-difluoro-2-phenylacetate → 2,2-Difluoro-2-phenylethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2,2-difluoro-2-phenylacetate | HCID 10631860 | — |
| Reactant | 2,2-Difluoro-4-phenylbutan-1-ol | HCID 18425775 | — |
| Product | 2,2-Difluoro-2-phenylethanol | HCID 9793891 | — |
Reaction Steps
Obtained from Intermediate 5 (13.2 g, 66 mmol) by the procedure described in Intermediate 2. The title compound was obtained (6.88 g, 66%) as oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420669B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-78a3a6239fea41b184544c74c906a751 |
| Source note | uspto-grants-2013_04 |