HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Difluoro-4-phenylbutan-1-ol → 2,2-Difluoro-2-(m-tolyl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Difluoro-4-phenylbutan-1-ol | HCID 18425775 | — |
| Reactant | Ethyl difluoro(3-methylphenyl)acetate | HCID 62394138 | — |
| Product | 2,2-Difluoro-2-(m-tolyl)ethanol | HCID 67245919 | — |
Reaction Steps
Obtained from Intermediate 28 (9.5 g, 40 mmol) by the procedure described in Intermediate 2. The title compound was obtained (5.55 g, 80%) as oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420669B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-3b57f3447caf4eaeaad13a10977b8a46 |
| Source note | uspto-grants-2013_04 |